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LIEBERMAN BOOKS

tppc

By Norman P. Lieberman

PROCESS ENGINEERING FACTS, FICTION AND FABLES

FIRST EDITION PUBLISHED BY: WILEY / SCRIVENER
ISBN 978-1-119-37027-7

CONTENTS

Other Books by Norman Lieberman   xiii
Introduction xv
Chapter 1. Process Operations & Design
Carl & Clare
3
Increasing Cooling Water Flow Thru an Elevated Condenser or Cooler
4

Hot Vapor By-Pass Pressure Control

7
Stalling A Thermosyphon Reboilers
10
Optimizing Fractionator Pressure
13

Adjusting Steam Turbine Speed to Minimize Steam Consumption

16
Steam Condensate Drainage from Reboilers Blowing Condensate Seal
19
Effect of Reflux on Fractionator Top Temperature
22

Centrifugal Pump Head Vs. Flow Performance Curves

25

Condensate Back-Up in Condensers – the Effect of Sub-Cooling

27

Distillation Tray Downcomer Back-Up and Liquid Flooding 

29
Effect of Foam on Level Indication in Distillation Towers 
32
Split Liquid Levels in Vertical Vapor – Liquid Separators 
35

Optimizing Excess Air in A Fired Heater to Minimize Fuel Consumption 

37
Distillation Tray Dumping or Weeping with Valve Cap Tray Decks
41

Fired Heater – Tube Failures

44

Low Air Flow in A Fin Fan Forced Draft Air Cooler

47
Measuring Air Flow for a Fin Fan Aerial Cooler
50
Measuring Cooling Tower Efficiency Approach to Wet Bulb Temperature
53

Adjusting Heater Stack Damper for Optimum Energy Efficiency 

56

Preventing Tray Dumping by Use of Bubble Cap Trays

59
Demister Fouling in Vapor-Liquid Separator Vessels 
62

Effect of Temperature on Liquid Level Indication

65
Draw-off Nozzle Capacity Limits 68
On-Stream Repair of Tube Leaks in Surface Condenser  70
When are Vortex Breakers Required? 73
Naphtha Injection to Centrifugal Compressor  76
Internal Overflow from Total Trap-Out Chimney Tray 80
Vacuum Ejector – Loose Steam Nozzle 
83
Effect of Tramp Air Leaks on Heater Efficiency 
86
Steam Turbine – Surface Condenser Outlet Temperature  92
Water Accumulation in Turbine Case 96
Chapter 2. Crude Distillation
Professor Pot & Kumar  
99
How to Adjust Pumparound Flows  100
How Top Reflux Rate Affects Flooding on Top Trays  103
Desalter – Adjusting Mix Valve Pressure Drop 107
Causes of Tray Deck Fouling   110
Minimizing Flash Zone Pressure  113
How to Adjust Bottoms Stripping Steam Rate 117
Overhead Condenser Corrosion  120
On-Line Spalling of Crude Pre-Heat Exchangers  123
Effect of Reflux on Overhead Accumulator Temperature 127
Removing Trays from Pre-Flash Towers  130
Total Trap – Out Chimney Tray  133
Side Draw-Off Limitations 136
Packed Towers  139
Rules of Thumb for Packed Towers  141
Controlling AGO Draw-Off Rate 143
Filming Amine Plugs Overhead Vapor Line  146
Stripping Tray Pressure Drop Profile  150
Protecting Crude Tower Stripping Trays from Damage Due to Water in Steam  153
Chapter 3. Engineering Basics
Irene & Norm 
157
Draft in Fired Heaters   158
Turbine Exhaust Surface Condenser Outlet Temperature 162
Adjusting Steam Turbine to Save Steam 166
Distillation Tray Downcomer Seal 170
Bernoulli’s Equation 173
Properties of Steam 176
Measuring Flows 179
Head Loss in Pipelines 182
Irene Explains Horsepower  185
Refrigeration 186
Packed Towers Vs. Trayed Towers  190
Condensing Steam Turbine Exhaust 194
Maximizing Lmtd in Heat Exchangers 198
Chapter 4. Routine Refinery Operating Problems
Dr. Petry & Pat
203
Pump Bearings Lubrication  204
Pressure Measurement Problems in Vapor Lines 207
Negative Pressure Drops 210
Coked-Up Thermowells 213
Centrifugal Compressor Surging  216
Commissioning Steam Turbine  219
Refrigeration Systems 222
Seal Pan Drain Hole  225
Measuring Steam Flow Without A Steam Meter  228
Air Leak on Suction of Cooling Water Pump 231
Chapter 5. Refinery  Safety
Dangerous Dan & Safety Sally 
235
Auto Ignition of Hydrocarbon 236
Failure of Mechanical Pump Seals  239
Sampling Tar Safely 242
Dangers of Iron Sulfides  244
H2S Fatalities  247
Fired Heater – Positive Pressure 250
Refinery Explosions & Fires  253
Flooding Fire Box with Fuel 256
Routing Relief Valves to the Flare 259
Isolating Equipment with Gate Valves  262
Explosive Limit of Hydrogen 265
Climate Change  268
Danger of Carbon Steel Piping Spool Pieces  271
Screwed Connections  274
Dangers of Steam Deaerators  277
Connecting Steam Hose to Hydrocarbon System 281
Process Vessel Collapse Under Vacuum During Start-Up  284
Acid Gas K.O. Drum   287
Safety Note 290
Value of a Chemical Engineering Degree to the Process Engineer in a Refinery 291
Chapter 6. Pitfalls in Computer Modeling 295
Basis for Process Engineering Calculations 296
Underlying Assumptions in Distillation Technology 297
Tray Fractionation Efficiency  298
Heat Exchanger Train Performance  299
Heat Exchanger Pressure Drop 300
Packed Towers  301
Air Coolers 302
Fired Equipment 303
Piping Systems 304
Centrifugal Pumps – NPSH   305
Rotating Equipment 306
Summary 307
References 308
Chapter 7. Latent Heat Transfer  309
Propane-Butane Splitter Reboiler 311
Heat Flux Limitations  312
Chapter 8. Hydraulics 315
Fluids other than Water 317
Rotational Energy 318
Pressure Drop Through an Orifice  319
Effect of Fluid Density on Orifice Pressure Drop 320
Head Loss in Piping 321
Factor Affecting Orifice Coefficients 323
Compressible Fluids 324
Chapter 9. Air Coolers  325
Measuring Air Flow 326
Air Recirculation 327
Vane Tip Clearance Problems 329
Cleaning Tube Bundle 330
Effect of Fouling on Reverse Air Flow 331
Effect of Adding Rows of Tubes  332
Changing Fan Blade Tips & Speed 333
Slipping Belts 334
Air Humidification 335
Induced Draft Fans  336
Chapter 10. Extracting Work from Steam  337
An Isentropic Expansion 338
Steam Turbines 339
The Potential Energy of Steam 340
Condensing  Steam at Low Pressure 342
The Meaning of Entropy 343
Video Library (list of videos) 345
The Norm Lieberman Refinery Troubleshooting Seminar on Video (details of program contents) 347
Index 349

(350 Numbered Pages Including the Index)
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